First direct synthesis of 4,8-dialkylbenzo[1,2-d;4,5-d′]bis[1,2,3]trithioles and 6,10-dialkyl[1,2,3]trithiolo[5,4-h]benzopentathiepins from 1,4-dialkyl-2,3,5,6-tetrabromobenzenes
Identifieur interne : 00BC50 ( Main/Exploration ); précédent : 00BC49; suivant : 00BC51First direct synthesis of 4,8-dialkylbenzo[1,2-d;4,5-d′]bis[1,2,3]trithioles and 6,10-dialkyl[1,2,3]trithiolo[5,4-h]benzopentathiepins from 1,4-dialkyl-2,3,5,6-tetrabromobenzenes
Auteurs : Ryu Sato ; Takeshi Kimura ; Takehiko Goto ; Minoru Saito ; Chizuko Kabuto [Japon]Source :
- Tetrahedron Letters [ 0040-4039 ] ; 1989.
English descriptors
- KwdEn :
- Ammonia, Calcd, Chem, Cyclic, Ethyl group, Lett, Polysulfides, Sato, Sulfur, Tetrahedron.
- Teeft :
- Ammonia, Calcd, Chem, Cyclic, Ethyl group, Lett, Polysulfides, Sato, Sulfur, Tetrahedron.
Abstract
Abstract: New cyclic polysulfides, 4,8-dialkylbenzo[1,2-d;4,5-d′]bis[1,2,3]-trithioles (2) and 6,10-dialkyl[1,2,3]trithiolo[5,4-h]benzopentathiepins (3), were directly synthesized by nucleophilic substitution of 1,4-dialkyl-2,3,5,6-tetrahalobenzenes (1) with elemental sulfur in liquid ammonia.
Url:
DOI: 10.1016/S0040-4039(00)99270-0
Affiliations:
Links toward previous steps (curation, corpus...)
- to stream Istex, to step Corpus: 005901
- to stream Istex, to step Curation: 005901
- to stream Istex, to step Checkpoint: 005824
- to stream Main, to step Merge: 00C402
- to stream Main, to step Curation: 00BC50
Le document en format XML
<record><TEI wicri:istexFullTextTei="biblStruct"><teiHeader><fileDesc><titleStmt><title>First direct synthesis of 4,8-dialkylbenzo[1,2-d;4,5-d′]bis[1,2,3]trithioles and 6,10-dialkyl[1,2,3]trithiolo[5,4-h]benzopentathiepins from 1,4-dialkyl-2,3,5,6-tetrabromobenzenes</title><author><name sortKey="Sato, Ryu" sort="Sato, Ryu" uniqKey="Sato R" first="Ryu" last="Sato">Ryu Sato</name></author><author><name sortKey="Kimura, Takeshi" sort="Kimura, Takeshi" uniqKey="Kimura T" first="Takeshi" last="Kimura">Takeshi Kimura</name></author><author><name sortKey="Goto, Takehiko" sort="Goto, Takehiko" uniqKey="Goto T" first="Takehiko" last="Goto">Takehiko Goto</name></author><author><name sortKey="Saito, Minoru" sort="Saito, Minoru" uniqKey="Saito M" first="Minoru" last="Saito">Minoru Saito</name></author><author><name sortKey="Kabuto, Chizuko" sort="Kabuto, Chizuko" uniqKey="Kabuto C" first="Chizuko" last="Kabuto">Chizuko Kabuto</name></author></titleStmt><publicationStmt><idno type="wicri:source">ISTEX</idno><idno type="RBID">ISTEX:B221FF0050E4DCFEFF42B25212DF02CE11F3AFBC</idno><date when="1989" year="1989">1989</date><idno type="doi">10.1016/S0040-4039(00)99270-0</idno><idno type="url">https://api.istex.fr/document/B221FF0050E4DCFEFF42B25212DF02CE11F3AFBC/fulltext/pdf</idno><idno type="wicri:Area/Istex/Corpus">005901</idno><idno type="wicri:explorRef" wicri:stream="Istex" wicri:step="Corpus" wicri:corpus="ISTEX">005901</idno><idno type="wicri:Area/Istex/Curation">005901</idno><idno type="wicri:Area/Istex/Checkpoint">005824</idno><idno type="wicri:explorRef" wicri:stream="Istex" wicri:step="Checkpoint">005824</idno><idno type="wicri:doubleKey">0040-4039:1989:Sato R:first:direct:synthesis</idno><idno type="wicri:Area/Main/Merge">00C402</idno><idno type="wicri:Area/Main/Curation">00BC50</idno><idno type="wicri:Area/Main/Exploration">00BC50</idno></publicationStmt><sourceDesc><biblStruct><analytic><title level="a">First direct synthesis of 4,8-dialkylbenzo[1,2-d;4,5-d′]bis[1,2,3]trithioles and 6,10-dialkyl[1,2,3]trithiolo[5,4-h]benzopentathiepins from 1,4-dialkyl-2,3,5,6-tetrabromobenzenes</title><author><name sortKey="Sato, Ryu" sort="Sato, Ryu" uniqKey="Sato R" first="Ryu" last="Sato">Ryu Sato</name></author><author><name sortKey="Kimura, Takeshi" sort="Kimura, Takeshi" uniqKey="Kimura T" first="Takeshi" last="Kimura">Takeshi Kimura</name></author><author><name sortKey="Goto, Takehiko" sort="Goto, Takehiko" uniqKey="Goto T" first="Takehiko" last="Goto">Takehiko Goto</name></author><author><name sortKey="Saito, Minoru" sort="Saito, Minoru" uniqKey="Saito M" first="Minoru" last="Saito">Minoru Saito</name></author><author><name sortKey="Kabuto, Chizuko" sort="Kabuto, Chizuko" uniqKey="Kabuto C" first="Chizuko" last="Kabuto">Chizuko Kabuto</name><affiliation wicri:level="4"><country xml:lang="fr">Japon</country><wicri:regionArea>Department of Chemistry, Faculty of Science, Tohoku University, Sendai 980</wicri:regionArea><orgName type="university">Université du Tōhoku</orgName><placeName><settlement type="city">Sendai</settlement><region type="province">Région de Tōhoku</region></placeName></affiliation></author></analytic><monogr></monogr><series><title level="j">Tetrahedron Letters</title><title level="j" type="abbrev">TETL</title><idno type="ISSN">0040-4039</idno><imprint><publisher>ELSEVIER</publisher><date type="published" when="1989">1989</date><biblScope unit="volume">30</biblScope><biblScope unit="issue">26</biblScope><biblScope unit="page" from="3453">3453</biblScope><biblScope unit="page" to="3456">3456</biblScope></imprint><idno type="ISSN">0040-4039</idno></series></biblStruct></sourceDesc><seriesStmt><idno type="ISSN">0040-4039</idno></seriesStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Ammonia</term><term>Calcd</term><term>Chem</term><term>Cyclic</term><term>Ethyl group</term><term>Lett</term><term>Polysulfides</term><term>Sato</term><term>Sulfur</term><term>Tetrahedron</term></keywords><keywords scheme="Teeft" xml:lang="en"><term>Ammonia</term><term>Calcd</term><term>Chem</term><term>Cyclic</term><term>Ethyl group</term><term>Lett</term><term>Polysulfides</term><term>Sato</term><term>Sulfur</term><term>Tetrahedron</term></keywords></textClass><langUsage><language ident="en">en</language></langUsage></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">Abstract: New cyclic polysulfides, 4,8-dialkylbenzo[1,2-d;4,5-d′]bis[1,2,3]-trithioles (2) and 6,10-dialkyl[1,2,3]trithiolo[5,4-h]benzopentathiepins (3), were directly synthesized by nucleophilic substitution of 1,4-dialkyl-2,3,5,6-tetrahalobenzenes (1) with elemental sulfur in liquid ammonia.</div></front></TEI><affiliations><list><country><li>Japon</li></country><region><li>Région de Tōhoku</li></region><settlement><li>Sendai</li></settlement><orgName><li>Université du Tōhoku</li></orgName></list><tree><noCountry><name sortKey="Goto, Takehiko" sort="Goto, Takehiko" uniqKey="Goto T" first="Takehiko" last="Goto">Takehiko Goto</name><name sortKey="Kimura, Takeshi" sort="Kimura, Takeshi" uniqKey="Kimura T" first="Takeshi" last="Kimura">Takeshi Kimura</name><name sortKey="Saito, Minoru" sort="Saito, Minoru" uniqKey="Saito M" first="Minoru" last="Saito">Minoru Saito</name><name sortKey="Sato, Ryu" sort="Sato, Ryu" uniqKey="Sato R" first="Ryu" last="Sato">Ryu Sato</name></noCountry><country name="Japon"><region name="Région de Tōhoku"><name sortKey="Kabuto, Chizuko" sort="Kabuto, Chizuko" uniqKey="Kabuto C" first="Chizuko" last="Kabuto">Chizuko Kabuto</name></region></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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